Table 1 Crystallographic data collection and refinement statistics.

X-ray crystallographic data for TrioC. Parentheses indicate values for highest resolution shell. ND, not determined; N/A, not available.

TrioCΔC (human Trio
1960–2275)
Data collection statistics
Synchrotron sourceLS-CAT beamline 21-ID-G,
advanced photon source
Wavelength (Å)0.97856
Resolution range (Å)50–2.65 (2.70–2.65)
Space groupP212121
Unit cell (a, b, c) (Å)59.2, 85.8, 182.4
Unique reflections30511 (1371)
Multiplicity5.0 (3.8)
Completeness (%)98.7 (90.1)
Mean I/σI18.9 (1.2)
CC1/2ND (0.699)
Rsym0.085 (0.746)
Refinement statistics
Resolution limits (Å)15–2.65 (2.70–2.65)
Number of test reflections28787 (1862)
Rwork0.23 (0.34)
Rfree0.27 (0.37)
Number of nonhydrogen atoms7525
  Macromolecule7499
  Ligand0
  Water26
Protein residues907
RMS bonds (Å)0.008
RMS angles (°)1.2
Ramachandran favored (%)97.8
Ramachandran outliers (%)0
Clashscore calculated from
MolProbity
1.33
Average B-factor76.0
  Macromolecule76.0
  LigandN/A
  Water48.0